3D Printed Microreactors for the Continuous Non?Kolbe Electrolysis
نویسندگان
چکیده
In the renaissance of organic electrochemistry, 150-year-old Kolbe chemistry offers a sustainable pathway to liquid energy carriers and commodities. Herein, easy-access design methods for electrochemical microreactors employing 3D printing simple post processing techniques are presented. The continuous Non-Kolbe electrolysis monomethyl succinic acid is studied as test reaction production an industrially relevant, green monomer. semi-batch setup, methyl acrylate produced with maximum yield 34 %, similar results from thoroughly optimized batch in prior study. single-pass experiments, comparable faradaic efficiency 54 % achieved.
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ژورنال
عنوان ژورنال: Chemie Ingenieur Technik
سال: 2022
ISSN: ['0009-286X', '1522-2640']
DOI: https://doi.org/10.1002/cite.202100178